[NMRFAM enews] May NMRFAM Newsletter - 2012

Rita Hannah rhannah at wisc.edu
Tue Apr 17 13:24:16 CDT 2012


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Description: Description: NMRFAM e-news

National Magnetic Resonance Facility at Madison

May 2012 time requests:

This is a reminder that April 19 @ 4pm CST, is the deadline for requesting
spectrometer time in May 2012 at NMRFAM.

++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
+++++++++++++++

.     The NMRFAM Protein Structure workshop will be held June 3rd to June
8th.
Information and a link for registration is available on the
<http://www.nmrfam.wisc.edu/home/workshops/> NMRFAM website .

.     Please note that you are now being charged for NMR tubes used in the
sample changer. You are requested to complete the template sheet with your
name and date so that we know when and for how many tubes to bill you. We do
not have any free tubes available and therefore the necessary change.

.     Please note that you are charged for time on the spectrometer if not
canceled 24 hours in advance of start time.

.     Gelbvieh (800 MHz) spectrometer is currently running on the triple
resonance room temperature probe.

.     Small Angle X-ray Scattering (SAXS):

.         Bruker-Axs Nanostar with a rotating anode source (funding obtained
from NIH-shared instrumentation - Prof. Sam Butcher-PI) is installed and
initial data sets have been collected.

.     A loaner 4mm 1H{X} cpmas probe (15,000 rpm max) has been installed on
the Bruker 500II (Devon) and is available by special request. This
instrument has solids amplifiers and is capable of many modern solids
experiments.

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+++++++++++++++

Spectrometers at NMRFAM:

.     Status of spectrometers can be determined at anytime as follows: In
Sundial after login, go to "Options"----->"Site
Resources"----->"Spectrometers" A new set of Options open on the Sundial
Board. Go to "Search"------>"By Owner". A new window pops up in the second
section (Manufacturer), type/write in either "Bruker " or "Varian". A
listing of the spectrometers will be displayed. Select the one of interest
and check on it's status, probes available etc.

.     NMRFAM instrumentation

Spectrometer status:


Instrument

 <http://www.nmrfam.wisc.edu/?page_id=500> Cow name

Shortcut name

Probe(a)

Status


Varian VNS 900

Fleckvieh

900

c-tr

OK-cold 1H and 13C preamps


Varian VNS 800

Gelbvieh

800

rt-tr

Ok


Bruker AV III 750

Telemark

750

c-tr

Ok


Bruker AV III 700

Rotvieh

700

c-qr
1H{13C,15N,31P}

OK-SampleJet


Bruker AV III 600

Dexter

600 I

c-qr
1H{13C,15N,31P}

OK-SampleJet


Varian VNS 600

Jaulan

600 II

c-tr

OK


Varian VNS 600

Vosges

600 III

c-tr

OK


Bruker AV III 600

Kurgan

600 IV

c-tr (1.7mm)

OK-SampleJet(cooled)


Bruker AV III 500

Kerry

500 I

c-tr(13C/15N)

OK-all cold preamp; Samplejet


Bruker AV III 500

Devon

500 II

c-tr/hrmas/BBFO/cpmas

OK - swappable CP
(solids capability)


Bruker DMX 400

Pisa

400

Multiple

OK


(a) rt - room temperature; c - cryogenic; tr - 1H{13C,15N} triple resonance;
qr - 1H{13C,15N,31P} quadruple resonance ; multiple - multiple probes; VNS-
Varian Direct Drive console; AV- Bruker Avance III console

To sign up for time: Use Sundial at

 <http://www.nmrfam.wisc.edu/home/schedule-nmr-time-sundial-2/>
http://www.nmrfam.wisc.edu/home/schedule-nmr-time-sundial-2/

Contact Rita Hannah ( <mailto:rhannah at nmrfam.wisc.edu>
rhannah at nmrfam.wisc.edu, 608-262-3173) for assistance. For scientific
questions/discussions contact Milo Westler ( <mailto:milo at nmrfam.wisc.edu>
milo at nmrfam.wisc.edu)

Please visit the  <http://www.nmrfam.wisc.edu/> NMRFAM website for more
information.

++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
+++++++++++

 

 

Rita Hannah, Ph.D.

NMRFAM

University of Wisconsin - Madison

Madison, WI - 53706

e-mail:  <mailto:rhannah at nmrfam.wisc.edu> rhannah at nmrfam.wisc.edu

Phone; (608) 262-3173

FAX: (608) 262-3759

 

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