[NMRFAM enews] NMRFAM September 2009
Milo Westler
milo at nmrfam.wisc.edu
Fri Sep 11 10:00:41 CDT 2009
[image: NMRFAM
e-news]<http://www.nmrfam.wisc.edu/wp-content/uploads/2009/09/enews_header.gif>
National
Magnetic Resonance Facility at Madison October 2009 time requests
This announcement is to remind you that September* 19th* @ 4pm is the
deadline for requesting spectrometer time in October 2009 at NMRFAM.
Recent developments:
- Visit our website @ www.nmrfam.wisc.edu and check the News on the right
side.
- The 13C/15N direct observe cryogenic probe has been installed on Kerry
(500I)- a 500 MHz Bruker Avance III with Samplejet. The signal-to-noise for
13C is 1400:1 (ASTM) and for 15N 80:1 (formamide). It is still suitable
for 1H observation (S/N 1600:1 Ethylbenzene). This spectrometer is
available for users.
- A Bruker Avance III 600 MHz LC-MS-NMR and a 700 MHz NMR spectrometer
are on order. They are expected to be delivered early 2010. The 600 MHz
spectrometer will have a LC-MS system for characterization and isolation of
metabolites and natural products and will be delivered with 5mm 1H{13C/15
N/31P} and 1.7mm 1H{13C/15N} cryogenic probes. The 700 MHz instrument
will have a 5mm 1H{13C/15N/31P} cryogenic probe. Both systems will have
SampleJet sample changers.
- See the YouTube videos describing rNMR <http://rnmr.nmrfam.wisc.edu/>,
the new small molecule visualization and quantification tool.
NMRFAM instrumentation Instrument *Cow name* Shortcut name Probe(a) Status
(09/11/2009) Varian VNS 900 Fleckvieh 900 c-tr OK (cold 1H and 13C
preamps) Varian
VNS 800 Gelbvieh 800 c-tr OK Bruker DMX 750 Telemark 750 c-tr under
repair Bruker
DMX 600 Dexter 600 I c-tr OK Varian VNS 600 Jaulan 600 II c-tr OK Bruker
Avance 500 Kerry 500 I Multiple OK- Avance III
console with 13C/15N observe cryogenic probe & SampleJet Bruker DMX 500
Devon 500 II c-tr OK Bruker DMX 400 Pisa 400 Multiple OK (a) rt - room
temperature; c - cryogenic; tr - 1H{13C,15N} triple resonance; multiple -
multiple probes; VNS- Varian Direct Drive; console Avance- Bruker Avance III
console
*To sign up for time:* Use Sundial at
www.sesame.wisc.edu/Sundial/sundial_main.html. Contact Anne Lynn
Gillian-Daniel (gillian at nmrfam.wisc.edu, 608-262-3173) for assistance.
Please visit the NMRFAM website for more information about
NMRFAM<http://www.nmrfam.wisc.edu/>
.
--
-- Milo
===================================================
National Magnetic Resonance Facility at Madison
An NIH-Supported Resource Center
W. Milo Westler, Ph.D.
NMRFAM Director
Senior Scientist
and
Adjunct Professor
433 Babcock Drive
Department of Biochemistry
University of Wisconsin-Madison
Madison, WI USA 53706-1544
EMAIL: milo at nmrfam.wisc.edu
PHONE: (608)-263-9599
FAX: (608)-263-1722
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